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- W263277532 abstract "A new improved synthesis of 2-deoxy-2-(/sup 18/F)fluoro-D-glucose (2-/sup 18/FDG, 4) from /sup 18/F-labeled acetyl hypofluorite (1) is described. Reaction of 3,4,6-tri-O-acetyl-D-glucal (2) with 1, generated in situ from (/sup 18/F)F/sub 2/ and ammonium acetate in acetic acid solution at room temperature, gave 2-deoxy-2-(/sup 18/F)fluoro-1,3,4,6-tetra-O-acetyl-..cap alpha..-D-glucopyranose (3). Hydrolysis of compound 3 with 2N HCl gave 2-deoxy-2-(/sup 18/F)fluoro-D-glucose (4) in radiochemical yields of approx.20% in a synthesis time of 70 min from EOB." @default.
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- W263277532 date "1982-10-01" @default.
- W263277532 modified "2023-09-23" @default.
- W263277532 title "New improved synthesis of 2-deoxy-2-(/sup 18/F)fluoro-d-glucose from /sup 18/F-labeled acetyl hypofluorite" @default.
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