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- W26345481 abstract "This chapter covers the different features of a powder diffraction pattern, which can be exploited in the characterization of a material. Powder diffraction data is most commonly used as a fingerprint in the identification of a material, but the other information that can be gleaned from a diffraction pattern should not be forgotten. If the pattern is to be indexed it is essential that the peak positions be determined accurately. In this case, the instrument's 2Θ scale needs to be carefully calibrated using a standard material such as the NIST silicon standard 640b. The sharper a peak, the better its 2Θ value can be determined, so the diffractometer should also be adjusted to optimize resolution. For indexing purposes, the intensities of the peaks are irrelevant, but for identification or for structure analysis, accurate relative intensities are essential. Most powder diffraction data analyses assume that the sample consists of millions of randomly oriented crystallites. If this is not the case, relative intensities will be distorted. In a zeolite laboratory, powder diffraction data are most commonly used to identify a newly synthesized material or to monitor the effects of a post-synthesis treatment." @default.
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- W26345481 date "2001-01-01" @default.
- W26345481 modified "2023-10-14" @default.
- W26345481 title "Product characterization by x-ray powder diffraction" @default.
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- W26345481 doi "https://doi.org/10.1016/b978-044450703-7/50107-1" @default.
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