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- W2685361785 abstract "Abstract Incorporating metal ions into a calcium hydroxyapatite structure is a successful pathway to increase their physical, chemical and biological properties. The calcium hydroxyapatite was obtained by co-precipitation and a hydrothermal-assisted sol-gel method at a low temperature, using Ca(NO 3 ) 2 ·4H 2 O and (NH 4 ) 2 HPO 4 as sources of calcium and phosphorus. Metal ion (M + = Mn 2+ , Fe 3+ , Co 2+ , Ni 2+ , Cu 2+ , Zn 2+ ) incorporation was carried out in solutions of calcium hydroxyapatite and the corresponding nitrate salts. Hydroxyapatite powders doped with metal ions were characterized by X-ray diffraction and FTIR analysis to evaluate the structural and compositional changes. The only phase present in pure and doped calcium hydroxyapatite samples (M + = Mn 2+ , Fe 3+ , Ni 2+ ) was the hexagonal one. A Rietveld refinement showed that doping with these ions does not affect the volume of the hexagonal unit cell. Both hexagonal and monoclinic phases were found in the samples doped with Co 2+ , Cu 2+ and Zn 2+ ions; however, we found that incorporating Zn 2+ into calcium hydroxyapatite stabilizes only the monoclinic phase." @default.
- W2685361785 created "2017-06-30" @default.
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- W2685361785 date "2017-10-01" @default.
- W2685361785 modified "2023-10-16" @default.
- W2685361785 title "Structural analysis of metal-doped (Mn, Fe, Co, Ni, Cu, Zn) calcium hydroxyapatite synthetized by a sol-gel microwave-assisted method" @default.
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- W2685361785 doi "https://doi.org/10.1016/j.ceramint.2017.06.154" @default.
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