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• W2718649311 startingPage "1028" @default.
• W2718649311 abstract "This study reports in situ observations of the formation of the δ′-ZrO phase, occurring during the annealing of transmission electron microscopy (TEM) thin foils of both pure Zr and a Zr–Sn–Nb–Mo alloy at 973 K in a transmission electron microsope. The lattice parameters of δ′-ZrO were measured and determined to be similar to those of the ω-Zr phase. The orientation relationship between the δ′-ZrO and α-Zr phases has been identified as either {(11 overline{2}0)}_{rm ZrO}//{(0002)}_{alpha} and {[0002]}_{rm ZrO}//{[11 overline{2}0]}_{alpha} or {(overline{1}011)}_{rm ZrO}//{(0002)}_{alpha} and {[01{overline 1}1]_{{rm{ZrO}}}}//{[11{overline 2}0]_alpha} depending on the orientation of the α grain relative to the TEM thin-foil normal. The nucleation and growth of δ′-ZrO were dynamically observed. This study suggests a new and convenient way to study oxidation mechanisms in Zr alloys and provides a deeper understanding of the properties of the newly reported δ′-ZrO. Since δ′-ZrO has a Zr sublattice which is identical to that of ω-Zr, the orientation relationships between the α and δ′-ZrO phases may also shed light on the orientation relations existing between α- and ω-Zr, and hence α- and ω-Ti." @default.
• W2718649311 created "2017-06-30" @default.
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• W2718649311 date "2017-06-26" @default.
• W2718649311 modified "2023-09-27" @default.
• W2718649311 title "<i>In situ</i>transmission electron microscopy study of the thermally induced formation of δ′-ZrO in pure Zr and Zr-based alloy" @default.
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• W2718649311 doi "https://doi.org/10.1107/s160057671700680x" @default.
• W2718649311 hasPublicationYear "2017" @default.
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