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- W2718822866 abstract "A hybrid organo- and biocatalytic system for the asymmetric conversion of racemic alcohols into amines was developed. Combining an organocatalyst, AZADO, an oxidant, NaOCl, and an enzyme, ω-transaminase, we implemented a one-pot oxidation–transamination sequential process in aqueous medium. The method showed broad substrate scope and was successfully applied to conventional secondary alcohols and sterically hindered β-substituted cycloalkanols, where a highly stereoselective dynamic asymmetric bioamination enabled us to set up both contiguous stereocenters with very high enantio- and diastereomeric ratio (>90% yield, >99% ee, and up to 49:1 dr)." @default.
- W2718822866 created "2017-06-30" @default.
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- W2718822866 date "2017-06-19" @default.
- W2718822866 modified "2023-10-18" @default.
- W2718822866 title "Hybrid Organo- and Biocatalytic Process for the Asymmetric Transformation of Alcohols into Amines in Aqueous Medium" @default.
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- W2718822866 doi "https://doi.org/10.1021/acscatal.7b01543" @default.
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