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• W2724865989 abstract "A telescoped procedure for the direct preparation of an advanced intermediate towards noroxymorphone from the naturally occurring alkaloids oripavine and thebaine is presented. The reaction procedure involves an intensified continuous‐flow hydroxylation, followed by a continuous solvent switch and hydrogenation in a packed‐bed hydrogenator (H‐Cube). The obtained reaction mixture, containing oxymorphone as intermediate in excellent yield and purity, can be then directly converted into the desired noroxymorphone oxazolidine intermediate through palladium catalyzed N ‐methyl oxidation." @default.
• W2724865989 created "2017-07-14" @default.
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• W2724865989 date "2017-08-14" @default.
• W2724865989 modified "2023-10-13" @default.
• W2724865989 title "An Integrated Continuous-Flow Synthesis of a Key Oxazolidine Intermediate to Noroxymorphone from Naturally Occurring Opioids" @default.
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• W2724865989 doi "https://doi.org/10.1002/ejoc.201700811" @default.
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