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- W2725420716 abstract "The unsaturated analogue of EDOT, 3,4-vinylenedioxythiophene (VDOT), is synthesized in a remarkable 55% yield in three steps from commercially available 3,4-dimethoxythiophene. The key step utilizes an efficient ruthenium-mediated ring-closing metathesis (RCM) reaction of electron-rich vinyl ethers (W. A. L. van Otterlo, E. L. Ngidi, C. B. de Koning Tetrahedron Lett. 2003, 44, 6483-6486). The dimer, BVDOT, was prepared via oxidative coupling of VDOT. Although BVDOT was successfully electropolymerized, the authors suggest that radical cation delocalization to the alkene in VDOT inhibits its electropolymerization." @default.
- W2725420716 created "2017-07-14" @default.
- W2725420716 date "2006-03-24" @default.
- W2725420716 modified "2023-10-14" @default.
- W2725420716 title "Ring-Closing Metathesis Approach to 3,4-Vinylenedioxythiophenes" @default.
- W2725420716 doi "https://doi.org/10.1055/s-2006-932062" @default.
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