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• W2726345975 abstract "A ditopic 18-membered N2O2S2-macrocycle (L) incorporating hard (NO2) and soft (NS2) binding sites in each side was employed and its three complexes (1–3) exhibiting different stoichiometries, geometries, and topologies have been prepared and structurally characterized. First, nickel(II) nitrate hexahydrate reacts with L to give a mononuclear complex [Ni(L)](NO3)2·2H2O (1) in which the metal center locates inside the macrocyclic cavity adopting a hexa-coordinated octahedral geometry shielded by the strongly bound macrocycle from the anion and solvent. While, silver(I) tetrafluoroborate afforded a one-dimensional coordination polymer {[Ag(L)]BF4}n (2) with an L-Ag-L-Ag pattern. In 2, the silver(I) center is penta-coordinate with NO donors from one L and NS2 donors from an adjacent L to form a sandwich-type adopting a distorted trigonal bipyramidal geometry. Mercury(II) chloride yielded a dinuclear complex [Hg2(L)Cl4] (3) in which two mercury(II) ions locate opposite side of L in a chair form. Each mercury(II) center in 3 is penta-coordinate, being bound to one pyridine N atom, two O(S) donors in the compositional disorder, and two chloride ions adopting a distorted square-pyramidal geometry. The comparative NMR studies show the preferential binding affinity of silver(I) over potassium(I) toward L." @default.
• W2726345975 created "2017-07-14" @default.
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• W2726345975 date "2017-09-01" @default.
• W2726345975 modified "2023-10-16" @default.
• W2726345975 title "Mononickel(II), dimercury(II), and 1-D polymeric silver(I) complexes with a ditopic 18-membered N2O2S2-macrocycle" @default.
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• W2726345975 doi "https://doi.org/10.1016/j.inoche.2017.06.029" @default.
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