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• W2728532854 abstract "A zirconium/nickel-mediated one-pot synthesis of ketones is reported. In the presence of Zn or Mn, Cp2ZrCl2 was found to dramatically accelerate the coupling and suppress side product formation via an I→SPy displacement at the same time. Unlike Zn/Pd- and Fe/Cu-mediated one-pot ketone syntheses, the new method is effective for nucleophiles bearing OR or equivalent functional groups at the α-position. A mechanism comprising a nickel catalytic cycle, a zirconium catalytic cycle, and Zr→Ni transmetalation is proposed, and Cp2ZrCl2 and/or low-valent Zr species are suggested to play crucial dual roles." @default.
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• W2728532854 date "2017-07-28" @default.
• W2728532854 modified "2023-10-01" @default.
• W2728532854 title "Zirconium/Nickel-Mediated One-Pot Ketone Synthesis" @default.
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• W2728532854 doi "https://doi.org/10.1002/anie.201705520" @default.
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