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- W2733274387 abstract "An efficient approach for synthesizing chiral β-amino nitroalkanes has been developed via the Ni-catalyzed asymmetric hydrogenation of challenging β-amino nitroolefins under mild conditions, affording the desired products in excellent yields and with high enantioselectivities. This protocol had good compatibility with the wide substrate scope and a range of functional groups. The synthesis of chiral β-amino nitroalkanes on a gram scale has also been achieved. In addition, the reaction mechanism was elucidated using a combined experimental and computational study, and it involved acetate-assisted heterolytic H2 cleavage followed by 1,4-hydride addition and protonation to achieve the nitroalkanes." @default.
- W2733274387 created "2017-07-14" @default.
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- W2733274387 date "2017-01-01" @default.
- W2733274387 modified "2023-10-04" @default.
- W2733274387 title "Nickel-catalyzed asymmetric hydrogenation of β-acylamino nitroolefins: an efficient approach to chiral amines" @default.
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- W2733274387 doi "https://doi.org/10.1039/c7sc02669b" @default.
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