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- W2736164810 abstract "TiO2 anatase was prepared by a novel preparation approach, combining utilization of titanyl sulphate as a precursor and pressurized water processing. In addition, two different chemical methods for preparation were used – thermal hydrolysis and induced hydrolysis. The photoactivity of developed TiO2 was examined in two environmentally-prospective reactions: azo-dye AO7 photodiscoloration (oxidation) and N2O photodecomposition (reduction). It was revealed that during the processing the temperature has a crucial effect on TiO2 crystallization contrary to pressure. TiO2 anatase of smaller crystallite-size showed significantly higher photoactivity in AO7 photodiscoloration than TiO2 anatase of large crystallite-size. However, in N2O photodecomposition all synthesized materials showed comparable activity. While the TiO2 anatase crystallite-size and surface area are the determining properties in azo-dye AO7 photodiscoloration, the electronic band structure and recombination rate of electron and holes are determining in N2O photodecomposition. The correlation enabling the estimation of TiO2 anatase crystallite-size from Raman FWHMs was found as well." @default.
- W2736164810 created "2017-07-21" @default.
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- W2736164810 date "2017-11-01" @default.
- W2736164810 modified "2023-09-26" @default.
- W2736164810 title "Novel TiO2 prepared from titanyl sulphate by using pressurized water processing and its photocatalytic activity evaluation" @default.
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- W2736164810 doi "https://doi.org/10.1016/j.materresbull.2017.07.010" @default.
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