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• W2736546364 abstract "Herein we report on the optimized synthesis process of SnIP, the first inorganic double helix compound which shows high mechanical flexibility, a strong tendency for cleavage or delamination and intriguing electronic properties. In this work we analyzed the influence of SnI2 as a reaction promotor or mineralizer compound for the synthesis of SnIP. In previous studies Sn/SnI4 was used as a precursor and chemical transport agent for the SnIP synthesis but significant amounts of non-reacted tin halide (SnI2 and SnI4) remained after the formation of the target compound reducing its quality and yield. Significantly less tin halide residue can be observed which suggests a reduction of side-reactions. While the Sn/SnI4 couple works perfectly for the synthesis of the two-dimensional material phosphorene precursor black phosphorus the Sn/SnI2 couple is beneficial for the one-dimensional ternary polyphosphide SnIP. These results strongly encourage the theory of SnI2 as the important reaction intermediate in the synthesis of covalently-bonded polyphosphide substructures and element allotropes at elevated temperatures." @default.
• W2736546364 created "2017-07-31" @default.
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• W2736546364 date "2017-10-01" @default.
• W2736546364 modified "2023-09-25" @default.
• W2736546364 title "A yield-optimized access to double-helical SnIP via a Sn/SnI2 approach" @default.
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• W2736546364 doi "https://doi.org/10.1016/j.jcrysgro.2017.07.015" @default.
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