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• W2741756755 abstract "We automated radiochemical synthesis of 1-[11C]acetoacetate in a commercially available radiochemistry module, TRASIS AllInOne by [11C]carboxylation of the corresponding enolate anion generated in situ from isopropenylacetate and MeLi, and purified by ion-exchange column resins.1-[11C]acetoacetate was synthesized with high radiochemical purity (95%) and specific activity (~ 66.6 GBq/µmol, n = 30) with 35% radiochemical yield, decay corrected to end of synthesis. The total synthesis required ~ 16 min. PET imaging studies were conducted with 1-[11C]acetoacetate in vervet monkeys to validate the radiochemical synthesis. Tissue uptake distribution was similar to that reported in humans." @default.
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• W2741756755 date "2017-11-01" @default.
• W2741756755 modified "2023-10-16" @default.
• W2741756755 title "Automated synthesis of 1-[11C]acetoacetate on a TRASIS AIO module" @default.
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• W2741756755 doi "https://doi.org/10.1016/j.apradiso.2017.07.066" @default.
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