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• W2741832907 startingPage "1326" @default.
• W2741832907 abstract "Pure, isomorphic, round, and free-flowing dimethyl fumarate granules in a size range of 250–2000 μm were successfully produced directly from esterification through the three-in-one intensified process of three distinctive steps of reaction, crystallization, and spherical agglomeration (SA) in a 0.5 L sized jacketed glass stirred tank. Dimethyl fumarate was prepared by sulfuric acid catalyzed esterification of fumaric acid with methanol. The reaction temperature was below the maximum allowable limit of 65 °C as determined by reaction kinetics to avoid the runaway situation. The dissolution rate of primary crystals of dimethyl fumarate was inversely proportional to the particle size which was strongly affected by the antisolvent addition and temperature cooling schemes during crystallization. However, the dissolution rate of the round granules was mainly dependent on the exterior dimension of the granules and not so much on the primary crystal size inside the granules. The mechanical properties such as dens..." @default.
• W2741832907 created "2017-08-08" @default.
• W2741832907 creator A5015953475 @default.
• W2741832907 creator A5088332400 @default.
• W2741832907 date "2017-08-14" @default.
• W2741832907 modified "2023-10-03" @default.
• W2741832907 title "Round Granules of Dimethyl Fumarate by Three-in-One Intensified Process of Reaction, Crystallization, and Spherical Agglomeration in a Common Stirred Tank" @default.
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• W2741832907 doi "https://doi.org/10.1021/acs.oprd.7b00183" @default.
• W2741832907 hasPublicationYear "2017" @default.
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