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- W2743148253 abstract "To access the benzofuro[3,2-b]indoline scaffold of the natural product phalarine, we planned an NIS-mediated oxidative coupling of an N-acetyltryptamine derivative and a phenol. To control the regioselectivity of benzofuroindoline formation, the phenol was appended, before the cyclisation, at the 2-position of the indole ring through an optimised gram-scale C–H arylation. The indole nucleus was indeed oxidised at its 3-position, however, the cyclisation did not occur through the phenol but through the acetamide and a 4′,5′-dihydrospiro[indole-3,6′-[1,3]oxazine] was obtained instead of the benzofuro[3,2-b]indoline scaffold of the natural product." @default.
- W2743148253 created "2017-08-17" @default.
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- W2743148253 date "2017-05-18" @default.
- W2743148253 modified "2023-10-18" @default.
- W2743148253 title "Evaluation of an NIS-Mediated Oxidative Cyclisation of Phenol-Containing <i>N</i> -Acyltryptamine Precursors towards Phalarine: Synthesis of 4′,5′-Dihydrospiro[indole-3,6′-[1,3]oxazine]s" @default.
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- W2743148253 doi "https://doi.org/10.1002/ejoc.201601563" @default.
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