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• W2743681856 abstract "FIB/SEM nanotomography (FIB-nt) is a powerful technique for the determination and quantification of the three-dimensional microstructure in subsurface features. Often times, the microstructure of a sample is the ultimate determiner of the overall performance of a system, and a detailed understanding of its properties is crucial in advancing the materials engineering of a resulting device. While the FIB-nt technique has developed significantly in the 15 years since its introduction, advanced nanotomographic analysis is still far from routine, and a number of challenges remain in data acquisition and post-processing. In this work, we present a number of techniques to improve the quality of the acquired data, together with easy-to-implement methods to obtain “advanced” microstructural quantifications. The techniques are applied to a solid oxide fuel cell cathode of interest to the electrochemistry community, but the methodologies are easily adaptable to a wide range of material systems. Finally, results from an analyzed sample are presented as a practical example of how these techniques can be implemented." @default.
• W2743681856 created "2017-08-17" @default.
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• W2743681856 date "2018-01-01" @default.
• W2743681856 modified "2023-10-17" @default.
• W2743681856 title "Improving microstructural quantification in FIB/SEM nanotomography" @default.
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• W2743681856 doi "https://doi.org/10.1016/j.ultramic.2017.07.017" @default.
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