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• W2744355562 endingPage "955" @default.
• W2744355562 startingPage "948" @default.
• W2744355562 abstract "Pentalithium aluminate (β-Li5AlO4) and the corresponding iron-containing solid solution (Li5(Al1−xFex)O4) were synthetized by solid-state reaction. All the samples were characterized structural and microstructurally by X-ray diffraction, solid-state nuclear magnetic resonance, scanning electron microscopy, N2 adsorption-desorption and temperature-programmed desorption of CO2. Results showed that 30 mol% of iron can be incorporated into the β-Li5AlO4 crystalline structure at aluminum positions. Moreover, iron addition induced morphological and superficial reactivity variations. Li5(Al1−xFex)O4 samples chemisorbed CO2 between 200 and 700 °C, where the superficial chemisorption presented the highest enhancement, in comparison to β-Li5AlO4. Additionally, Li5(Al1−xFex)O4 samples sintered at higher temperatures than β-Li5AlO4. Isothermal CO2 chemisorption experiments of β-Li5AlO4 and Li5(Al1−xFex)O4 were fitted to a first order reaction model, corroborating that iron enhances the CO2 chemisorption, kinetically. When oxygen was added to the gas flow, CO2 chemisorption process was mainly enhanced between 400 and 600 °C for the Li5(Al0.8Fe0.2)O4 sample in comparison to β-Li5AlO4. Hence, Li5(Al1−xFex)O4 solid solution presented an enhanced CO2 chemisorption process, in the presence and absence of oxygen, in comparison to β-Li5AlO4." @default.
• W2744355562 created "2017-08-17" @default.
• W2744355562 creator A5003025277 @default.
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• W2744355562 date "2017-09-01" @default.
• W2744355562 modified "2023-10-03" @default.
• W2744355562 title "Synthesis and evaluation as CO2 chemisorbent of the Li5(Al1−Fe )O4 solid solution materials: Effect of oxygen addition" @default.
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• W2744355562 doi "https://doi.org/10.1016/j.jechem.2017.08.002" @default.
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