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- W2744634997 abstract "Abstract The visible‐light‐promoted decarboxylation of α‐imino‐oxy propionic acids for the generation of iminyl radicals has been accomplished through the use of Ir(dFCF 3 ppy) 2 (dtbbpy)PF 6 as a photoredox catalyst. Different from visible‐light‐promoted homolysis and single‐electron reduction of oxime derivatives, this strategy provides a novel catalytic cycle for alkene carboimination through a sequence comprising N‐radical generation, iminyl radical cyclization, intermolecular conjugate addition to a Michael acceptor, and single‐electron reduction to afford various pyrroline derivatives in an overall redox‐neutral process. The indolizidine alkaloid skeleton could be easily constructed from a pyrroline derivative prepared by this synthetic method." @default.
- W2744634997 created "2017-08-17" @default.
- W2744634997 creator A5014528157 @default.
- W2744634997 creator A5090922097 @default.
- W2744634997 date "2017-09-05" @default.
- W2744634997 modified "2023-10-17" @default.
- W2744634997 title "Iminyl‐Radicals by Oxidation of α‐Imino‐oxy Acids: Photoredox‐Neutral Alkene Carboimination for the Synthesis of Pyrrolines" @default.
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- W2744634997 doi "https://doi.org/10.1002/anie.201706270" @default.
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