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- W2748124224 abstract "A new chiral capillary electrophoresis (CE) analytical method for the determination of six pairs of amino acid enantiomer-derivatized precapillary with 9-fluorenylmethoxycarbonyl chloride (FMOC) was developed. CE separation parameters such as the pH of background electrolyte, the boric acid concentration, the addition of D-fructose and isopropanol, and the effect of new binary chiral selectors on the electropherograms were investigated. Precapillary and in-capillary derivatization was compared as well. The results showed that enantiomeric separations were obtained with enantio-resolution (Rs) ranged from 2.61 to 9.99 for the FMOC-derivatized amino acid enantiomers except alanine with Rs 1.06. Precapillary derivatization method provides overall better Rs for nearly all the targets except FMOC-aspartate with efficiency up to 1.309 × 106 plates and limit of detection (LOD) down to 2.5 μM. This method was successfully applied to analyze the concentration of the D/L-glutamic acid and D/L-aspartate in seven rice wine samples." @default.
- W2748124224 created "2017-08-31" @default.
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- W2748124224 date "2017-09-14" @default.
- W2748124224 modified "2023-10-14" @default.
- W2748124224 title "Enantioseparation of amino acids by micellar capillary electrophoresis using binary chiral selectors and determination of <scp>D</scp>-glutamic acid and <scp>D</scp>-aspartic acid in rice wine" @default.
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- W2748124224 doi "https://doi.org/10.1080/10826076.2017.1364263" @default.
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