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• W2748162384 abstract "Racemic 4-O-allyl-myo-inositol-1,3,5-orthoesters were resolved as the corresponding diastereomeric dicamphanates by crystallization from alcoholic solvents. Crystals of the two diastereomers of myo-inositol orthoacetate and one diastereomer each of myo-inositol orthoformate and myo-inositol orthobenzoate were obtained in >99% purity, on gram scale. The configuration of all these diastereomers was established by conversion to known chiral myo-inositol derivatives as well as by single crystal structure analysis. It is interesting to note that the procedures for the separation of diastereomeric myo-inositol orthoesters could be evolved due to the knowledge of crystal growth and crystal structures of inositol derivatives of comparable molecular structures. Due to the synthetic versatility of myo-inositol orthoesters, the methods described provide rapid and convenient access to a variety of chiral inositol derivatives with high synthetic potential." @default.
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• W2748162384 date "2017-09-07" @default.
• W2748162384 modified "2023-09-26" @default.
• W2748162384 title "Clues from Crystal Structures Pave the Way to Access Chiral <i>myo</i>-Inositol Derived Versatile Synthons: Resolution of Racemic 4-<i>O</i>-Allyl-<i>myo</i>-Inositol-1,3,5-Orthoesters via Corresponding Dicamphanates by Crystallization" @default.
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• W2748162384 doi "https://doi.org/10.1021/acs.cgd.7b00895" @default.
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