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- W2751322420 abstract "A variety of applications of 8‐alkynylated nucleosides has prompted the synthesis of new purine analogues. Bromination of unprotected 2‐amino‐2′‐deoxyadenosine with Br 2 /Ac OH /Ac ON a gives 2‐amino‐8‐bromo‐2′‐deoxyadenosine (87%). The brominated derivative is converted to 8‐alkynylated 2‐amino‐2′‐deoxyadenosines by palladium‐catalyzed Sonogashira cross‐coupling reaction via microwave assistance (81 – 95%). The resulting compounds are further transformed to 8‐alkynylated 2′‐deoxyisoguanosines (52 – 70%). The physical properties of new compounds are investigated." @default.
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- W2751322420 date "2017-12-27" @default.
- W2751322420 modified "2023-09-23" @default.
- W2751322420 title "Synthesis of 8-Substituted 2′-Deoxyisoguanosines<i>via</i>Unprotected 8-Brominated 2-Amino-2′-deoxyadenosine" @default.
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- W2751322420 doi "https://doi.org/10.1002/cbdv.201700335" @default.
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