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- W2753281609 abstract "A new procedure of microwave-assisted organic synthesis in flow was designed and introduced for Fischer indole synthesis of 7-ethyltryptophol (7-ET). By using back-pressure regulator (BPR), a reaction temperature of 180 °C could be easily and readily achieved even in a low-boiling solvent [water/ethylene glycol(EG)]. At this temperature, the synthesis of 7-ET from 2-ethylphenylhydrazine and 4-hydroxybutanal in flow was successful (78% net yield) and practical (short residence time: 30 s) with a simple purification process of extraction." @default.
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- W2753281609 date "2017-11-01" @default.
- W2753281609 modified "2023-10-18" @default.
- W2753281609 title "A continuous flow microwave-assisted fischer indole synthesis of 7-Ethyltryptophol" @default.
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- W2753281609 doi "https://doi.org/10.1016/j.cep.2017.09.001" @default.
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