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- W2754127922 abstract "The present work articulates the synthesis of a new series of organo‐functionalized triethoxysilanes derived from versatile carboxylic acids and 3‐azidopropyltriethoxysilane in excellent yields. A proficient and convenient route implicating the Cu(I)‐catalysed 1,3‐cycloaddition of organic azide with terminal alkynes, labelled as click silylation , has been developed for the generation of ester‐triazole‐linked alkoxysilanyl scaffolds ( 4a – f ). All the synthesized compounds have been thoroughly characterized using elemental analysis and Fourier transform infrared, 1 H NMR and 13 C NMR spectroscopic techniques. Importantly, the fabricated alkoxysilanes are potentially amenable for an in situ sol–gel condensation reaction with silica nanospheres leading to the incorporation of organic functionality via covalent grafting onto the nanostructured particle system. As a proof of concept, a one‐pot preparation of organic–inorganic hybrid nanoparticles is presented using bis‐silane 4 f . The efficiency and selectivity of the prepared nanocomposite towards metal ions is highlighted using adsorption experiments, and the immobilized nanoparticles present a high sensing efficiency towards Cu 2+ and Pb 2+ ions while demonstrating better response than that of the bulk material." @default.
- W2754127922 created "2017-09-25" @default.
- W2754127922 creator A5021708883 @default.
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- W2754127922 date "2017-09-15" @default.
- W2754127922 modified "2023-10-10" @default.
- W2754127922 title "An expedient ‘click’ approach for the synthetic evaluation of ester‐triazole‐tethered organosilica conjugates" @default.
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- W2754127922 doi "https://doi.org/10.1002/aoc.4028" @default.
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