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• W2754794294 abstract "The novel A2B2O7-type compound Pb2Co2O7 was synthesized at 8 GPa and 1673 K. Synchrotron X-ray diffraction shows a cubic pyrochlore structure with space group Fd3̅m. Rietveld structural analysis reveals a large cation mixed occupancy at both A and B sites by about 40%, the greatest value found in the pyrochlore family. In combination with the X-ray absorption spectroscopy results, the specific chemical composition and charge states are determined to be (Co0.6Pb0.4)3+2(Pb0.6Co0.4)4+2O7, in which both the A-site Co3+ and the B-site Co4+ are low-spin. Due to the tetrahedral geometric frustration effects as well as the random Co4+ and Pb4+ distribution at the B site, spin glassy behavior is well observed following the conventional critical slowing down feature in Pb2Co2O7." @default.
• W2754794294 created "2017-09-25" @default.
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• W2754794294 date "2017-09-18" @default.
• W2754794294 modified "2023-10-17" @default.
• W2754794294 title "High-Pressure Synthesis of the Cobalt Pyrochlore Oxide Pb₂Co₂O₇ with Large Cation Mixed Occupancy" @default.
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• W2754794294 doi "https://doi.org/10.1021/acs.inorgchem.7b01646" @default.
• W2754794294 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/28920686" @default.
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