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- W2755910324 abstract "Abstract Using high-resolution scanning tunneling microscopy (STM), we have studied the oxidation of rutile TiO 2 (1 1 0)–(1 × 1) surfaces with H ad species at room temperature. We followed the evolution of various stable species as function of the O 2 exposure, and the nature of the ultimately dominating species in the Ti troughs is described. When O 2 saturation was accomplished using a glass-capillary array doser, we found that on-top O (O ot ) adatoms are the predominant surface species. In contrast, when O 2 was supplied via backfilling of the chamber the predominant surface species are tentatively assigned to terminal OH groups. We argue that unintended reactions with the chamber walls have a strong influence on the formed surface species, explaining scattered results in the literature. On the basis of our STM data we propose an alternative, easy way of preparing oxidized TiO 2 (1 1 0) surfaces with O ot adatoms ( o -TiO 2 ). It is certain that o -TiO 2 (1 1 0) surfaces prepared according to this recipe do not have any residual surface O vacancies. This contradicts the situation when oxidizing reduced TiO 2 (1 1 0) surfaces with O vacancies, where some O vacancies persist." @default.
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- W2755910324 date "2017-12-01" @default.
- W2755910324 modified "2023-09-27" @default.
- W2755910324 title "A new recipe for preparing oxidized TiO2(1 1 0) surfaces: An STM study" @default.
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- W2755910324 doi "https://doi.org/10.1016/j.susc.2017.09.001" @default.
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