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• W275592011 abstract "ABSTRACT ：New coupling agent or surface modified agent (9-decenoic acid) was used to enhance the compatibility betweensilica and polystyrene in silica/polystyrene hybrid nanocomposite, synthesized by in situ miniemulsion polymerization. Composites contain well dispersed nanosize silica particles. Related tests and analyses confirmed the success of synthesis.Functionalization of silica by 9-decenoic acid and silica on the polystyrene was confirmed by FTIR. TGA showed presenceand amount of silica in final latex. The glass transition temperature of the hybrid nanocomposite was increased with thesilica amount. SEM and TEM analysis showed the spherical morphology of PS and composite with an average diameterof 55 nm. The presence of silica within composite was confirmed by EDS attached to the existing TEM.요 약：In situ 미니에멀젼 중합으로 실리카/폴리스타이렌 하이브리드 나노복합체를 만들기 위하여 9-데세노 산을실리카 표면 개질제로 처음 도입하였다. 복합체는 나노크기의 잘 분산된 실리카를 함유하고 있었다. 실리카의 표면 개질 및 폴리스타이렌의 합성 등은 FTIR로 확인하였고 생성 라텍스 중에 존재하는 실리카의 양은 TGA 분석으로확인하였다. 생성된 하이브리드는 실리카의 양 증가에 따라 유리전이온도가 상승하였다. SEM과 TEM으로 확인한 결과 하이브리드 복합체는 평균 직경이 55 nm 정도로 나타났다. 복합체내의 실리카의 존재는 EDS와 연결된 TE M 등으로 확인되었다." @default.
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• W275592011 date "2009-03-01" @default.
• W275592011 modified "2023-09-24" @default.
• W275592011 title "Synthesis and Characterization of Silica/Polystyrene Composite Nanoparticles by in situ Miniemulsion Polymerization" @default.
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