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- W2757325155 abstract "We report a simple procedure for rapid, visible light-mediated, controlled radical polymerization in aqueous solutions. Based on the photoelectron transfer reversible addition-fragmentation chain transfer (PET-RAFT) polymerization, fast chain propagation at room temperature in water was achieved in the presence of reductant and without prior deoxygenation. A systematic study correlating irradiation intensity and polymerization kinetics, enabled by in situ nuclear magnetic resonance spectroscopy, provided optimized reaction conditions. The versatility of this procedure was demonstrated through a rapid triblock copolymer synthesis, and incorporation of water-labile activated esters for direct conjugation of hydrophilic small molecules and proteins. In addition, this technique boasts excellent temporal control and provides a wide range of macromolecular materials with controlled molecular weights and narrow molecular weight distributions." @default.
- W2757325155 created "2017-10-06" @default.
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- W2757325155 date "2017-09-22" @default.
- W2757325155 modified "2023-10-11" @default.
- W2757325155 title "Rapid Visible Light-Mediated Controlled Aqueous Polymerization with In Situ Monitoring" @default.
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- W2757325155 doi "https://doi.org/10.1021/acsmacrolett.7b00587" @default.
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