Matches in SemOpenAlex for { <https://semopenalex.org/work/W2758995418> ?p ?o ?g. }
Showing items 1 to 59 of
59
with 100 items per page.
- W2758995418 abstract "The seed oil of Microula sikkimensis Hemsl. was extracted by supercritical carbon dioxide extraction,microwave-assisted re？ux extraction, ultrasound-assisted extraction and solvent re？ux extraction. The experimental parameters of supercritical carbon dioxide extraction which is classic in these extraction techniques including pressure, temperature, particle size and extraction time were optimized. A simple and sensitivemethod for the simultaneous determination of 39 kinds of saturated and unsaturated fatty acids in seed oil using high performance liquid chromatography (HPLC) with ？uorescence detection following pre-column derivatization with 1-[2-(p-toluenesulfonate)-ethyl]-2-phenylimidazole-[4,5-f]-9,10-phenanthrene (TSPP) has been developed. Fatty acid derivatives were separated on a reversed-phase Eclipse XDB-C8 column in conjunctionwith a gradient elution. Quantitative linear range of 39 fatty acids was 0.014–14.29 mmol/L, and excellent linear responses were observed with correlation coef？cients more than 0.9992. Detection limits were in the range of 3.24–36.97 fmol (10 mL, S/N3:1). Stability of derivatives, method repeatability and recovery were evaluated and the results were excellent for ef？cient HPLC analysis. Fatty acids in M. sikkimensis Hemsl. seed oil with or without saponi？cation by different extraction methods were analyzed and compared. The facile TSPP derivatization coupled with HPLC ？uorescence detection allowed for the quantitation of short- and long-chain fatty acids from biological and natural environmental samples." @default.
- W2758995418 created "2017-10-06" @default.
- W2758995418 creator A5006183780 @default.
- W2758995418 creator A5084723028 @default.
- W2758995418 date "2010-01-01" @default.
- W2758995418 modified "2023-09-24" @default.
- W2758995418 title "Extraction of Microula sikkimensis seed oil and simultaneous analysis of saturated and unsaturated fatty acids by ？uorescence detection with reversed-phase HPLC" @default.
- W2758995418 hasPublicationYear "2010" @default.
- W2758995418 type Work @default.
- W2758995418 sameAs 2758995418 @default.
- W2758995418 citedByCount "0" @default.
- W2758995418 crossrefType "journal-article" @default.
- W2758995418 hasAuthorship W2758995418A5006183780 @default.
- W2758995418 hasAuthorship W2758995418A5084723028 @default.
- W2758995418 hasConcept C134458231 @default.
- W2758995418 hasConcept C154020017 @default.
- W2758995418 hasConcept C179998833 @default.
- W2758995418 hasConcept C185592680 @default.
- W2758995418 hasConcept C2776923573 @default.
- W2758995418 hasConcept C43617362 @default.
- W2758995418 hasConcept C4725764 @default.
- W2758995418 hasConcept C81426234 @default.
- W2758995418 hasConceptScore W2758995418C134458231 @default.
- W2758995418 hasConceptScore W2758995418C154020017 @default.
- W2758995418 hasConceptScore W2758995418C179998833 @default.
- W2758995418 hasConceptScore W2758995418C185592680 @default.
- W2758995418 hasConceptScore W2758995418C2776923573 @default.
- W2758995418 hasConceptScore W2758995418C43617362 @default.
- W2758995418 hasConceptScore W2758995418C4725764 @default.
- W2758995418 hasConceptScore W2758995418C81426234 @default.
- W2758995418 hasIssue "1" @default.
- W2758995418 hasLocation W27589954181 @default.
- W2758995418 hasOpenAccess W2758995418 @default.
- W2758995418 hasPrimaryLocation W27589954181 @default.
- W2758995418 hasRelatedWork W1971146327 @default.
- W2758995418 hasRelatedWork W1976492461 @default.
- W2758995418 hasRelatedWork W2041090299 @default.
- W2758995418 hasRelatedWork W2047915670 @default.
- W2758995418 hasRelatedWork W2050936702 @default.
- W2758995418 hasRelatedWork W2054980445 @default.
- W2758995418 hasRelatedWork W2056714700 @default.
- W2758995418 hasRelatedWork W2060095269 @default.
- W2758995418 hasRelatedWork W2166853230 @default.
- W2758995418 hasRelatedWork W2355012662 @default.
- W2758995418 hasRelatedWork W2358565263 @default.
- W2758995418 hasRelatedWork W2366340817 @default.
- W2758995418 hasRelatedWork W2374760374 @default.
- W2758995418 hasRelatedWork W2390853777 @default.
- W2758995418 hasRelatedWork W2394025800 @default.
- W2758995418 hasRelatedWork W2500133701 @default.
- W2758995418 hasRelatedWork W2525919700 @default.
- W2758995418 hasRelatedWork W2568333871 @default.
- W2758995418 hasRelatedWork W2621057557 @default.
- W2758995418 hasRelatedWork W3152432237 @default.
- W2758995418 hasVolume "23" @default.
- W2758995418 isParatext "false" @default.
- W2758995418 isRetracted "false" @default.
- W2758995418 magId "2758995418" @default.
- W2758995418 workType "article" @default.