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• W2760692040 endingPage "2014" @default.
• W2760692040 startingPage "2010" @default.
• W2760692040 abstract "The mechanochemical Knoevenagel condensation of malononitrile with p -nitrobenzaldehyde was studied in situ using a tandem approach. X-ray diffraction and Raman spectroscopy were combined to yield time-resolved information on the milling process. Under solvent-free conditions, the reaction leads to a quantitative conversion to p -nitrobenzylidenemalononitrile within 50 minutes. The in situ data indicate that the process is fast and proceeds under a direct conversion. After stopping the milling process, the reaction continues until complete conversion. The continuous and the stopped milling process both result in crystalline products suitable for single crystal X-ray diffraction." @default.
• W2760692040 created "2017-10-06" @default.
• W2760692040 creator A5048636019 @default.
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• W2760692040 date "2017-09-26" @default.
• W2760692040 modified "2023-10-15" @default.
• W2760692040 title "Mechanochemical Knoevenagel condensation investigated in situ" @default.
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• W2760692040 doi "https://doi.org/10.3762/bjoc.13.197" @default.
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