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• W2761293722 abstract "The new hybrid [4-Cl-2-(CH3)C6H3NH3]6P6O18·2H2O was synthesized under normal conditions of temperature and pressure. Single crystal X-ray diffraction study was used to identify its structure. It revealed that this organic cyclohexaphosphate crystallized in the P1¯ triclinic space group with a = 10.41 (10) Å b = 10.94 (7) Å, c = 15.45 (10) Å, α = 77.37 (8), β = 89.75 (8)°, γ = 61.69 (7)°, V = 1501 (2) Å3 and Z = 1. In the crystal framework, the assembling of the three dimensional (3D) structure is formed by intermolecular hydrogen bonds and Van Der Waals interactions. A spectroscopic characterization was carried out to elucidate the structure (UV–Vis, FTIR, 31P MAS-NMR and fluorescent properties). The thermal stability was studied by TG-DTA diagrams under argon atmosphere. Furthermore, 3-D Hirshfeld surfaces in combination with 2-D fingerprint plots were carried out. This compound was also evaluated for its antioxidant activity; four tests were done, in vitro, 1,1-diphenyl-2-picrylhydrazyl (DPPH•), hydroxyl scavenging ability (OH•), ferric reducing power (FRP) and ferrous ion chelating (FIC) ability, using ascorbic acid as a control." @default.
• W2761293722 created "2017-10-20" @default.
• W2761293722 creator A5039161827 @default.
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• W2761293722 date "2018-02-01" @default.
• W2761293722 modified "2023-09-25" @default.
• W2761293722 title "Synthesis, structural analysis, Hirshfeld surface, spectroscopic characterization and, in vitro , antioxidant activity of a novel organic cyclohexaphosphate" @default.
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• W2761293722 doi "https://doi.org/10.1016/j.molstruc.2017.10.031" @default.
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