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- W276277572 abstract "Silicon nitride ceramics with the grain-boundary phase {beta}-eucryptite, LiAlSiO{sub 4}, or {beta}-spodumene, LiAlSi{sub 2}O{sub 6}, were produced by pressureless sintering {alpha}-Si{sub 3}N{sub 4}, SiO{sub 2}, and LiAlO{sub 2} powder mixtures at 1,300{degree} to 1,900{degree}C. The phase relations in the system Si{sub 3}N{sub 4}-LiAlO{sub 2}-SiO{sub 2} were investigated at 1,500{degree}C, showing the presence of an Si-Li-O rich liquid phase. During annealing at 900{degree} to 1,300{degree}C, {beta}-eucryptite precipitated when the sintering temperature was 1,700{degree}C. Because of the low thermal expansion of {beta}-LiAlSiO{sub 4} and {beta}-LiAlSi{sub 2}O{sub 6} ({minus}6.3 {times} 10{sup {minus}7}{degree}C{sup {minus}1} and 8.3 {times} 10{sup {minus}7}{degree}C{sup {minus}1}, RT = 1,000{degree}C), thermal-induced misfit stresses will be developed. Because of these stresses, toughening effects can be expected in the composite microstructures." @default.
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- W276277572 date "1987-10-01" @default.
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- W276277572 title "Formation and Characteristics of Silicon Nitride-Lithium Aluminum Silicate Ceramics: Part I, Sintering and Microstructure" @default.
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- W276277572 doi "https://doi.org/10.1111/j.1551-2916.1987.tb00154.x" @default.
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