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- W2763973237 abstract "We have synthesized Ba2NaNb5O15 (BNN) crystal by annealing 25.6BaO-6.4Na2O–32Nb2O5– 24SiO2–12B2O3 (BNNSB) glass and investigated the crystallization kinetics from the glass. The glass sample was prepared by a plate quenching method. Thermal, structural, vibrational and surface properties have been studied by using differential thermal analysis, X-ray diffraction, Raman spectroscopy and atomic force microscopy, respectively. It is found that the grain sizes of the orthorhombic Ba2NaNb5O15 crystal occurred in the BNNSB glass are confined within 30~50 nm. The isothermal model of the Johnson-Mehl-Avrami-Kolmogorov function is applied to characterize the kinetics of the crystallization process. The Avrami exponent 4.5 indicates that the crystallization mechanism belongs to an increasing nucleation rate with the interface-controlled growth. The activation energy of crystallization, 5.0 eV, obtained from the isothermal model, show the similar value to that resulted from the isoconversion method. The Raman scatte..." @default.
- W2763973237 created "2017-10-20" @default.
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- W2763973237 date "2017-10-18" @default.
- W2763973237 modified "2023-10-17" @default.
- W2763973237 title "Formation of Ba2NaNb5O15 Crystal and Crystallization Kinetics in BaO–Na2O–Nb2O5–SiO2–B2O3 Glass" @default.
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- W2763973237 doi "https://doi.org/10.1021/acs.cgd.7b00576" @default.
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