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• W2765200310 abstract "A silver- and copper-free rhodium-catalyzed C–H acetoxylation reaction of azaindoles has been achieved at near ambient temperature employing PIDA as a nonmetallic acetoxy source. The method is highly selective, efficient, and scalable and requires acetic anhydride as the sole additive. The scope of the reaction has been successfully tested with a wide array of medicinally important heterocyclic scaffolds with diverse functional group tolerance. A series of kinetic experiments was conducted to gain detailed insight into the reaction mechanism. The methodology developed could be successfully expanded for C7-acetoxylation of indoline derivatives using pyrimidine as a detachable directing group for the synthesis of 7-hydroxyindole." @default.
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• W2765200310 date "2017-11-07" @default.
• W2765200310 modified "2023-10-14" @default.
• W2765200310 title "Rhodium-Catalyzed sp² C–H Acetoxylation of <i>N</i>-Aryl Azaindoles/<i>N</i>-Heteroaryl Indolines" @default.
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• W2765200310 doi "https://doi.org/10.1021/acs.joc.7b02203" @default.
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