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• W2765332392 endingPage "13077" @default.
• W2765332392 startingPage "13070" @default.
• W2765332392 abstract "La24Sr14–7x[Si36N72](O1–xFx)14 with x = 0.489 was obtained as a microcrystalline product by metathesis at 1500 °C in a radio-frequency furnace starting from Si(NH)2, La(NH2)3, SrH2, LaF3, and CeF3. The structure of the new nitridosilicate oxide fluoride was determined by combining transmission electron microscopy (TEM) and single-crystal X-ray diffraction using a microfocused synchrotron beam. The structure model with pronounced disorder [P63/mmc, Z = 1, a = 16.2065(3), c = 9.4165(1) Å, R1(obs) = 0.0436] was confirmed by electron diffraction and aberration-corrected Z-contrast scanning TEM. The highly symmetric AB2 framework, which was theoretically predicted but not yet realized, consists of all-side vertex-sharing SiN4 tetrahedra that form channels along [001] filled with La, Sr, O, and F atoms. The connectivity pattern is related to that of tridymite. X-ray spectroscopy and bond-valence-sum calculations were further taken into account for assignment of the N, O, and F atoms." @default.
• W2765332392 created "2017-11-10" @default.
• W2765332392 creator A5007237901 @default.
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• W2765332392 date "2017-10-17" @default.
• W2765332392 modified "2023-10-01" @default.
• W2765332392 title "Highly Symmetric AB₂ Framework Related to Tridymite in the Disordered Nitridosilicate La₂₄Sr_{14–7<i>x</i>}[Si₃₆N₇₂](O_1–<i>x</i>F_<i>x</i>)₁₄ (<i>x</i> = 0.489)" @default.
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• W2765332392 doi "https://doi.org/10.1021/acs.inorgchem.7b01862" @default.
• W2765332392 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29039656" @default.
• W2765332392 hasPublicationYear "2017" @default.
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