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• W2765402468 abstract "Bromoporphyrins were prepared by the metal-mediated self-condensation of brominated 1-formyldipyrromethanes. Depending on the conditions, Mg(II)-2,12-dibromoporphyrin and Mg(II)-2-bromoporphyrin could be obtained in up to 11% and 17% isolated yield, respectively. Zn(II) was also a viable templating metal. The positions of the bromine substituents were confirmed by 2D-NMR spectroscopic analysis and the X-ray crystal structure of a derivative. Suzuki and Sonogashira reactions of the bromoporphyrins yielded 2-substituted or 2,12-disubstituted porphyrins with red-shifted absorption and emission spectra. This method provides access to the minimalist core of β-mono- and β,β'-disubstituted porphyrins from readily available starting materials." @default.
• W2765402468 created "2017-11-10" @default.
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• W2765402468 date "2017-11-15" @default.
• W2765402468 modified "2023-09-25" @default.
• W2765402468 title "Rational Synthesis of 2-Bromoporphyrins and 2,12-Dibromoporphyrins" @default.
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• W2765402468 doi "https://doi.org/10.1021/acs.joc.7b02404" @default.
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