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- W2765698966 abstract "The iron-catalyzed oxidative activation of the (O)CC bond in ketones has been developed. This method enables direct synthesis of esters by the reaction between ketones and alcohols via conversion of the (O)CC bond to the (O)CO bond. The reaction runs selectively: the (O)CCAlkyl bond is activated, while the (O)CCAryl bond remains intact (i.e., iron-catalyzed intermolecular anti-Baeyer-Villiger activation of the (O)CC bond). The reaction conditions are carefully optimized and allow the production of esters with yields of up to 95%. The method is based on the inexpensive and commercially available catalyst (FeCl3), oxidant ((NH4)2S2O8), and solvent (DCE) without using any ligands or additives." @default.
- W2765698966 created "2017-11-10" @default.
- W2765698966 creator A5033132890 @default.
- W2765698966 date "2017-12-01" @default.
- W2765698966 modified "2023-09-23" @default.
- W2765698966 title "Iron-catalyzed C C bond activation/C O bond formation: Direct conversion of ketones to esters" @default.
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- W2765698966 doi "https://doi.org/10.1016/j.tetlet.2017.10.068" @default.
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