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- W2767053721 abstract "In a detailed study, the influence of microwave irradiation, synthesis time and temperature, addition of acetic acid (HAc) as a modulator on the morphology, crystallinity and stability of UiO-66-NH2 is investigated to develop a reliable and reproducible strategy for the preparation of well-shaped UiO-66-NH2. The UiO-66-NH2 were characterized by powder X-ray diffraction (PXRD), field emission scanning electron microscopy (FESEM), thermogravimetric analysis (TGA), and gas adsorption. It is found that well-shaped UiO-66-NH2 with a high CO2 adsorption capacity can be synthesized in a short time by microwave heating. The UiO-66-NH2 crystals synthesized by microwave heating are of high quality and show a superior CO2 adsorption capacity (5.8 mmol/g at 273k and 1 bar) due to the strong interactions between the −NH2 group and CO2. The CO2/N2 selectivity of the obtained UiO-66-NH2 at 298 K and 1 bar is 66, which is much higher than that of the pristine UiO-66 of 17.8." @default.
- W2767053721 created "2017-11-10" @default.
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- W2767053721 date "2018-02-01" @default.
- W2767053721 modified "2023-09-27" @default.
- W2767053721 title "Microwave-assisted synthesis of well-shaped UiO-66-NH2 with high CO2 adsorption capacity" @default.
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- W2767053721 doi "https://doi.org/10.1016/j.materresbull.2017.10.038" @default.
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