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- W2767402495 abstract "The Cu dispersed on mesoporous SBA-15 has demonstrated the regioselective CH bond C3-cyanation of indoles by in-situ generation of CN using DMF and NH4I in presence of O2. Pyridine adsorbed diffuse reflectance infrared spectroscopy (DRIFTS) results revealed that surface Cu2+ species are acting as Lewis acid sites in the in-situ generation of cyano- group for the synthesis of indole nitriles. A direct correlation between Cu metal surface area and the indole nitrile yields are established and the dual role of copper is substantiated by N2O titration and XPS techniques. The 10 wt%Cu/SBA-15 demonstrated superior performance when compared to Pd, Ru supported on SBA-15. The 10 wt%Cu/SBA-15 catalyst showed consistent activity and selectivity after the 4th cycle." @default.
- W2767402495 created "2017-11-17" @default.
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- W2767402495 date "2018-02-01" @default.
- W2767402495 modified "2023-09-27" @default.
- W2767402495 title "An insight on the influence of surface Lewis acid sites for regioselective C H bond C3-cyanation of indole using NH4I and DMF as combined cyanide source over Cu/SBA-15 catalyst" @default.
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- W2767402495 doi "https://doi.org/10.1016/j.mcat.2017.11.007" @default.
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