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- W2767544273 abstract "As one of the important bone regeneration materials, α-calcium sulfate hemihydrate (α-CSH) has attracted widespread attention. In this study, a facile method was developed to prepare α-CSH with low aspect ratio via high-gravity continuously reactive precipitation of a calcium sulfate dihydrate (CSD) precursor, using ethanol as a morphology modifier in a rotating packed bed (RPB) reactor, combined with CaCl2 salt solution method under atmospheric pressure with the addition of citric acid with a low concentration (0.06 wt %). The precipitation time of CSD powders in the RPB was dramatically shortened from 30 min to 1 s, and the precursor exhibited more regular short rod shapes and much smaller size, compared to that obtained in a conventional stirring tank reactor (STR). Furthermore, calcium sulfate bone materials with high stability and good mechanical property were prepared by mixing α-CSH and normal saline with a liquid–solid ratio of 0.6. The RPB products had a higher compressive strength (2–3 times) than the STR counterpart." @default.
- W2767544273 created "2017-11-17" @default.
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- W2767544273 date "2017-11-15" @default.
- W2767544273 modified "2023-10-15" @default.
- W2767544273 title "Facile Preparation of α-Calcium Sulfate Hemihydrate with Low Aspect Ratio Using High-Gravity Reactive Precipitation Combined with a Salt Solution Method at Atmospheric Pressure" @default.
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- W2767544273 doi "https://doi.org/10.1021/acs.iecr.7b03356" @default.
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