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- W2767708370 abstract "Abstract Cationic gold(I) complexes with hollow‐shaped triethynylphosphine ligands efficiently catalyzed intramolecular [2+2] cycloaddition of 1,9‐enynes to afford cyclobutene‐fused eight‐membered carbocycles that were difficult to synthesize by other catalytic systems. Various 1,9‐enynes with carbon linkers with or without a fused ring underwent efficient [2+2] cycloaddition with 5 mol% of the Au catalyst bearing the triarylmethyl‐end‐capped triethynylphosphine in CH 2 Cl 2 at rt in the presence of MS 4A as an additive. More challenging 1,9‐enyne substrates with fully saturated acyclic carbon linkers underwent eight‐membered ring formation at 60 °C in ClCH 2 CH 2 Cl in the absence of MS 4A, forming monocyclic 1,3‐dienes as major products. magnified image" @default.
- W2767708370 created "2017-11-17" @default.
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- W2767708370 date "2017-12-13" @default.
- W2767708370 modified "2023-10-14" @default.
- W2767708370 title "Synthesis of Cyclobutene‐Fused Eight‐Membered Carbocycles through Gold‐Catalyzed Intramolecular Enyne [2+2] Cycloaddition" @default.
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- W2767708370 doi "https://doi.org/10.1002/adsc.201701193" @default.
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