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- W2768620113 abstract "Two complementary cascade cyclization reactions, namely, the KHSO 4 ‐promoted [1+2+3] cyclization and the TMSCl‐promoted four‐component cascade cyclization, are described for the concise synthesis of highly functionalized spirooxindoles in excellent yields. The improved TMSCl‐promoted cyclization reaction of isatins, N , N ‐dimethylenaminones, and amines was carried out under milder conditions than those of the [1+2+3] cyclization to afford the desired products. The observed chemoselectivity of this TMSCl‐promoted cyclization is explained by the design and preparation of an intermediate bis(enaminone). A gram‐scale synthesis and synthetic applications of this transformation were also evaluated." @default.
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- W2768620113 date "2017-12-29" @default.
- W2768620113 modified "2023-10-13" @default.
- W2768620113 title "Two Complementary Cyclization Reactions for the Chemoselective Synthesis of Spirooxindoles" @default.
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- W2768620113 doi "https://doi.org/10.1002/ejoc.201701413" @default.
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