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- W2769057973 abstract "A method for the synthesis of diversely substituted 3-fluoropyridines from two ketone components is described. The reaction involves photoredox coupling of α,α-difluoro-β-iodoketones with silyl enol ethers catalyzed by fac-Ir(ppy)3 under blue LED irradiation with subsequent one-pot condensation with ammonium acetate. Based on cyclic voltammetry studies, it was determined that α,α-difluoro-β-iodoketones are reduced notably easier compared to 2,2,2-trifluoro-1-iodoethane, which may be ascribed to the influence of the carbonyl group." @default.
- W2769057973 created "2017-12-04" @default.
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- W2769057973 date "2017-11-30" @default.
- W2769057973 modified "2023-09-27" @default.
- W2769057973 title "Synthesis of 3-Fluoropyridines via Photoredox-Mediated Coupling of α,α-Difluoro-β-iodoketones with Silyl Enol Ethers" @default.
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- W2769057973 doi "https://doi.org/10.1021/acs.joc.7b02467" @default.
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