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- W2769269500 abstract "This paper describes the application of a novel antisolvent crystallization approach to rapid production of tunable solid solutions of hydrophobic amino acids, comprising l-leucine, l-isoleucine, and l-valine. The antisolvent approach provides an alternative to other crystallization routes, e.g., ball-milling, liquid-assisted grinding, and slurry methods, to achieve the required multicomponent solid phases. We report new crystal structures of l-leucine/l-isoleucine and l-leucine/l-valine, and confirm a recent report on a new form of l-isoleucine/l-valine. We used these multicomponent complexes as a test set of materials to demonstrate translation of small scale batch antisolvent crystallization to a continuous production process." @default.
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- W2769269500 date "2017-12-18" @default.
- W2769269500 modified "2023-10-15" @default.
- W2769269500 title "Rapid Continuous Antisolvent Crystallization of Multicomponent Systems" @default.
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- W2769269500 doi "https://doi.org/10.1021/acs.cgd.7b01105" @default.
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