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- W2769630770 abstract "Extracts obtained from whole annatto seeds were fractionated with supercritical carbon dioxide using a home-made experimental apparatus. The crude extracts, obtained in a 100 mL extractor at 313 K and 20 MPa were fractionated in two separator vessels, i.e., S-1 operating at 312 K and 9 MPa, and S-2 operating at 282 K and 4 MPa. Chemical composition of the resulted products was evaluated in terms of a qualitative approach using thin-layer chromatography. High-pressure phase behavior experiments were applied to the fractionated extracts using a synthetic-visual apparatus. Results indicate that annatto extracts were successfully fractionated in terms of visual aspects and differences in chemical profile. Chemical composition suggest that annatto extracts present relevant profile of terpenes and phenolics. The extracts presented similar phase behavior with the occurrence of vapor–liquid-equilibria, and vapor–liquid–liquid phase behavior for the studied compositions." @default.
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- W2769630770 date "2017-01-01" @default.
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- W2769630770 title "Fractionation of Annatto Extracts with Carbon Dioxide Using a Home-Made Equipment" @default.
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