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- W2770295563 endingPage "6311" @default.
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- W2770295563 abstract "A visible-light photoredox cleavage of α-allenylic C-O bond and alkenyl C-S formation is disclosed for the first time. The thiolation of allenyl phosphine oxides with diaryl disulfides occurs smoothly in metal-free and mild conditions, affording novel S,P-bifunctionalized butadienes with moderate to excellent yields. Mechanistic studies explain the cleavage of a C(sp3)-O(Ar) bond in initiating a key alkenyl radical intermediate." @default.
- W2770295563 created "2017-12-04" @default.
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- W2770295563 date "2017-11-20" @default.
- W2770295563 modified "2023-09-26" @default.
- W2770295563 title "Visible-Light-Driven α-Allenylic C–O Bond Cleavage and Alkenyl C–S Formation: Metal-Free and Oxidant-Free Thiolation of Allenyl Phosphine Oxides" @default.
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- W2770295563 doi "https://doi.org/10.1021/acs.orglett.7b03052" @default.
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