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• W2770361567 abstract "Research Article| December 01, 2017 SYNTHESIS OF A CHALCOGENIDE GLASS STANDARD FOR LASER ABLATION-INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY (LA-ICP-MS) Yanan Liu; Yanan Liu 1Department of Earth Sciences, University of Toronto, Toronto, Ontario M5S 3B1, Canada †Corresponding author: e-mail, liu@es.utoronto.ca Search for other works by this author on: GSW Google Scholar James M. Brenan; James M. Brenan 1Department of Earth Sciences, University of Toronto, Toronto, Ontario M5S 3B1, Canada2Department of Earth Sciences, Dalhousie University, Halifax, Nova Scotia B3H 3R2, Canada Search for other works by this author on: GSW Google Scholar Colin J. Bray Colin J. Bray 1Department of Earth Sciences, University of Toronto, Toronto, Ontario M5S 3B1, Canada Search for other works by this author on: GSW Google Scholar Author and Article Information Yanan Liu 1Department of Earth Sciences, University of Toronto, Toronto, Ontario M5S 3B1, Canada James M. Brenan 1Department of Earth Sciences, University of Toronto, Toronto, Ontario M5S 3B1, Canada2Department of Earth Sciences, Dalhousie University, Halifax, Nova Scotia B3H 3R2, Canada Colin J. Bray 1Department of Earth Sciences, University of Toronto, Toronto, Ontario M5S 3B1, Canada †Corresponding author: e-mail, liu@es.utoronto.ca Publisher: Society of Economic Geologists Accepted: 11 Aug 2017 First Online: 15 Nov 2017 Online Issn: 1554-0774 Print Issn: 0361-0128 © 2017 Economic GeologyEconomic Geology Economic Geology (2017) 112 (8): 2005–2021. https://doi.org/10.5382/econgeo.2017.4538 Article history Accepted: 11 Aug 2017 First Online: 15 Nov 2017 Cite View This Citation Add to Citation Manager Share Icon Share Facebook Twitter LinkedIn MailTo Tools Icon Tools Get Permissions Search Site Citation Yanan Liu, James M. Brenan, Colin J. Bray; SYNTHESIS OF A CHALCOGENIDE GLASS STANDARD FOR LASER ABLATION-INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY (LA-ICP-MS). Economic Geology 2017;; 112 (8): 2005–2021. doi: https://doi.org/10.5382/econgeo.2017.4538 Download citation file: Ris (Zotero) Refmanager EasyBib Bookends Mendeley Papers EndNote RefWorks BibTex toolbar search Search Dropdown Menu toolbar search search input Search input auto suggest filter your search All ContentBy SocietyEconomic Geology Search Advanced Search Abstract We demonstrate the synthesis of a chalcogenide (~Ge30Sb10S60) glass, suitable as a standard for laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) analysis of platinum group elements (PGEs), chalcogens (Se, As, Te, Sb, and Bi), transition metals (Co, Fe, Cr, Mn, Ni, Cu, and Zn), and other elements (Mo, W, Sn, Pb, and Ga). The synthesis was accomplished by subjecting the sample, vacuum sealed in a fused silica ampoule, to melting (Tmax of 950°–975°C) then quenching over a total period of ~30 h. The method allows for the synthesis of a relatively large sample (~10 g, in this report) of homogeneous glass with good laser coupling characteristics. Doped concentrations were ~100 μg/g for most elements, except for Ru, Os, Re, W, and Mo, which were homogeneous only when added at the 5- to 10-μg/g level. The trace element homogeneity of the glasses was verified by LA-ICP-MS, and the absolute concentrations were determined using both solution and LA-ICP-MS. Accuracy of the chalcogenide glass as a standard to measure other matrices was verified by analyses of silicate and sulfide reference materials, with results in accord with accepted values for most of the elements considered. You do not have access to this content, please speak to your institutional administrator if you feel you should have access." @default.
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• W2770361567 title "SYNTHESIS OF A CHALCOGENIDE GLASS STANDARD FOR LASER ABLATION-INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY (LA-ICP-MS)" @default.
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