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- W2775561396 abstract "Purpose: This work aims to functionalize the commercial glass ionomer by sol-gel process, to improve the physicochemical properties of the ionomer. Methods: The commercial glass ionomer SS White - Vidrion F, was pretreatment with HCl acid and base NaOH diluted, separately. The functionalization was carried out through the sol-gel process with the addition in a 50.0 mL flask, 50 mg of ionomer, 12.0 mL of ethyl alcohol, 2.0 mL distilled water and 0.5 mL of the 3- (trimethoxysilyl) propyl methacrylate alkoxide, the flask is connected to a ball condenser connected to a thermostatic bath with water circulation, the suspension was remained under stirring for 24 h at 80 ° C. The final product was centrifuged, washed and dried in an oven at 50 ° C under reduced pressure. Results: The infrared spectra presents a new bands in the carbonate region, besides the presence of bands of groups C=O and C=C, characteristics of the alkoxide, this is an indication of the functionalization of the samples. The diffractograms presented the same patterns described in the literature for the ionomer used, which suggests a cubic crystalline system, corroborating with the results obtained through vibrational spectroscopy. Conclusion: Characterization techniques show that the different treatments may influence the glass ionomer matrix and consequently the functionalization, but the results obtained were satisfactory. The glass ionomer was functionalized in both treatment with NaOH and HCl." @default.
- W2775561396 created "2017-12-22" @default.
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- W2775561396 date "2017-09-27" @default.
- W2775561396 modified "2023-09-26" @default.
- W2775561396 title "SOL-GEL PROCESS AS TOOLS FOR FUNCTIONALIZATION GLASS IONOMER" @default.
- W2775561396 doi "https://doi.org/10.26843/investigacao.v16i7.2144" @default.
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