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- W2775707942 abstract "A strategy for rapid screening for the separation of chiral molecules of pharmaceutical interest by normal-phase liquid chromatography using three cellulose/amylose stationary phases is proposed. In a first step, the most important parameters for the separations were determined and studied for their effects by means of experimental designs. Results showed that the cellulose tris-(3,5-dimethylphenylcarbamate), the amylose tris-(3,5-dimethylphenylcarbamate) and the cellulose tris-(4-methylbenzoate) stationary phases have very broad and complementary enantiorecognition properties. The type of organic modifier used in the mobile phase appeared to have a dramatic influence on the quality of the separation. Based on the results of the preliminary study, a screening strategy was developed and successfully applied to a set of 36 diverse drugs. Enantiomeric separation was observed in 89% of cases and the analysis times were usually shorter than 20 min." @default.
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- W2775707942 date "2002-02-01" @default.
- W2775707942 modified "2023-10-12" @default.
- W2775707942 title "Screening approach for chiral separation of pharmaceuticals" @default.
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- W2775707942 doi "https://doi.org/10.1016/s0021-9673(01)01573-4" @default.
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