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• W2775744079 abstract "The main goal of this work was to investigate, in a systematic way, the influence of the controlled modulation of the particle size distribution of a representative solid sample with respect to the more relevant analytical parameters of the Direct Solid Analysis (DSA) by Total-reflection X-Ray Fluorescence (TXRF) quantitative method. In particular, accuracy, uncertainty, linearity and detection limits were correlated with the main parameters of their size distributions for the following elements; Al, Si, P, S, K, Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, As, Se, Rb, Sr, Ba and Pb. In all cases strong correlations were finded. The main conclusion of this work can be resumed as follows; the modulation of particles shape to lower average sizes next to a minimization of the width of particle size distributions, produce a strong increment of accuracy, minimization of uncertainties and limit of detections for DSA-TXRF methodology. These achievements allow the future use of the DSA-TXRF analytical methodology for development of ISO norms and standardized protocols for the direct analysis of solids by mean of TXRF." @default.
• W2775744079 created "2017-12-22" @default.
• W2775744079 creator A5016902996 @default.
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• W2775744079 date "2018-02-01" @default.
• W2775744079 modified "2023-09-26" @default.
• W2775744079 title "Effect of modulation of the particle size distributions in the direct solid analysis by total-reflection X-ray fluorescence" @default.
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• W2775744079 doi "https://doi.org/10.1016/j.sab.2017.12.007" @default.
• W2775744079 hasPublicationYear "2018" @default.
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