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- W2778130473 abstract "The reaction of Ni(mnt)2 (mnt = 1,2-dicyano-1,2-ethylenedithiolate) with CuI in THF results in the formation of a Ni(mnt)2Cu4I4 unit with an eight-membered Cu4I4 crown motif. Coordination polymers with Ni(mnt)2Cu4I4 building units, having doubly bridged 1-D chains, were formed with bulky NBu4 counterions. To pack the bulky NBu4 cations into the crystal structure, no direct interactions between the 1-D chain structures are observed. When the bulky NBu4 cations are exchanged for small sodium cations, direct interactions between the 1-D chain structures dominate. A doubly bridged 2-D sheet structure is formed through the bridging of the cyano groups of the Ni(mnt)2Cu4I4 units of neighboring 1-D chain structures by sodium atoms. The monomeric [Na2(18-crown-16)]2[Ni(mnt)2Cu4I4] complex is formed when the sodium cations of the 2-D sheet structure are captured by 18-crown-6. The configuration of the coordination polymer or the monomer is controlled through the selection of the appropriate countercation to the Ni..." @default.
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- W2778130473 date "2017-12-26" @default.
- W2778130473 modified "2023-10-18" @default.
- W2778130473 title "Controlled Self-Assembly of a 2-D Sheet Coordination Polymer and Monomer Containing an Eight-Membered Cu4I4 Crown Motif" @default.
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- W2778130473 doi "https://doi.org/10.1021/acs.cgd.7b01440" @default.
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